(1. 中南大學(xué) 材料科學(xué)與工程學(xué)院，長沙 410083；
2. 中南大學(xué) 粉末冶金國家重點(diǎn)實(shí)驗(yàn)室，長沙 410083；
3. 中南大學(xué) 有色金屬材料科學(xué)與工程教育部重點(diǎn)實(shí)驗(yàn)室，長沙 410083)
摘 要: 采用實(shí)驗(yàn)觀察和理論計算相結(jié)合研究經(jīng)多向鍛造后AZ80A 鎂合金等溫退火過程中的顯微組織演變與再結(jié)晶動力學(xué)。結(jié)果表明：經(jīng)多向鍛造后的AZ80A 鎂合金在150 ℃退火處理時，隨著退火時間的延長，再結(jié)晶晶粒逐漸增多，退火時間為3600 s 時，發(fā)生再結(jié)晶的體積分?jǐn)?shù)約為88%；175 ℃退火時，合金在1800 s 時已經(jīng)發(fā)生了完全再結(jié)晶，且有部分晶粒發(fā)生長大；200 ℃退火時，合金在360 s 時的再結(jié)晶體積分?jǐn)?shù)約為70%，900 s 時再結(jié)晶晶粒發(fā)生長大；250 ℃退火時，退火360 s 后，再結(jié)晶晶粒已經(jīng)發(fā)生了部分長大。利用Avrami 再結(jié)晶動力學(xué)方程計算可得到多向鍛造態(tài)AZ80A 鎂合金的再結(jié)晶激活能為71.48 kJ/mol，合金在150、175、200 和250 ℃退火時再結(jié)晶完成的時間分別為4160、1387、485 和85.6 s；計算結(jié)果與實(shí)驗(yàn)結(jié)果一致。
關(guān)鍵字: AZ80A 鎂合金；等溫退火；靜態(tài)再結(jié)晶；再結(jié)晶動力學(xué)；
（1. School of Materials Science and Engineering,Central South University,Changsha 410083,China;
2. State Key Laboratory of Powder Metallurgy,Central South University,Changsha 410083,China;
3. Key Laboratory of Nonferrous Metal Materials Science and Engineering,
Ministry of Education,Central South University,Changsha 410083,China）
Abstract:The microstructure evolution and the kinetics analysis of static recrystallization during annealing of multiple forged AZ80A magnesium alloy were studied by experimental observation and theoretical calculation. The results show that,with the extension of annealing time,the recrystallized grains increase gradually at the annealing time of 3600 s,the volume function of recrystallization is about 88% after annealing heat treatment at 150 ℃; when the annealing temperature is 175 ℃ and the annealing time is 1800 s,the fully static recrystallization occurs and some grains grow up; at the annealing temperature of 200 ℃,the volume fraction of recrystallized grains is about 70% at the annealing time of 360 s,and some of the recrystallied grains grow up at annealing time of 900 s. At the temperature of 250 ℃,the recrytallized grains grow up after 360 s. Based on the Avrami kinetics analysis of static recrystallization process,the full recrystallization times at 150,175,200 and 250 ℃ are 4160,1387,485 and 85.6 s,respectively. The recrystallization energy for multiple forged AZ80A magnesium alloy is 71.48 kJ/mol,and calculated results are consistent with the experimental ones.
Key words: AZ80A magnesium alloy; isothermal annealing; static recrystallization; recrystallization kinetics
