Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中國有色金屬學(xué)報(bào)

ZHONGGUO YOUSEJINSHU XUEBAO

第23卷    第7期    總第172期    2013年7月

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文章編號(hào):1004-0609(2013)07-1873-06
(Fe-Cr)(40)-Al(60)摻雜鎢精礦粉激光燒結(jié)合金組織及性能
李 剛,韓 鳳,沈 宇,沈金澤,王 妍

(遼寧工程技術(shù)大學(xué) 材料科學(xué)與工程學(xué)院,阜新 123000)

摘 要: 往(Fe-Cr)(40)-Al(60)粉末中加入1%(質(zhì)量分?jǐn)?shù))的鎢精礦粉,利用激光引燃自蔓延燒結(jié)制備原位自生顆粒增強(qiáng)復(fù)合材料。通過SEM、XRD等微觀組織結(jié)構(gòu)表征手段及合金密度、孔隙率、硬度、磨損性能等宏觀力學(xué)性能及腐蝕性能測試的方法,研究不同引燃功率對(duì)燒結(jié)合金組織及性能的影響。結(jié)果表明:燒結(jié)合金物相主要為AlFe、AlFe3、Al2O3、Al65Fe20W15、W及硬質(zhì)顆粒相WO3。燒結(jié)合金組織為針片狀,且隨功率的增加,組織變得均勻細(xì)密。當(dāng)功率達(dá)到1 100 W時(shí),燒結(jié)合金密度最大,為4.47 g/cm3,孔隙率最小,為4.43%;硬度最高,表層區(qū)達(dá)到1 309.7HK,中部區(qū)達(dá)到1 003.1HK;合金耐蝕性能最好,鈍化區(qū)最長為440 mV,鈍化電流密度最小為5.570 μA/mm2。而當(dāng)燒結(jié)功率為1 000 W時(shí),試樣磨損率最低,表層區(qū)為0.06 mg/mm2,中部區(qū)為0.05 mg/mm2

 

關(guān)鍵字: Fe-Al金屬間化合物;激光燒結(jié);顯微組織;性能

Microstructure and properties of (Fe-Cr)(40)-Al(60) with tungsten concentrate powders by laser sintering
LI Gang, HAN Feng, SHEN Yu, SHEN Jin-ze, WANG Yan

College of Materials Science and Engineering, Liaoning Technical University, Fuxin 123000, China

Abstract:By putting 1% (mass fraction) tungsten concentrate powders into(Fe-Cr)(40)-Al(60) powders and using laser ignition induced SHS, the in situ antigenic particle reinforced composite alloy was prepared. By means of SEM, XRD, alloy density, porosity, hardness test, abrasion test and corrosion resistance, the effect of different ignition powers on the sintered alloy microstructure and properties was studied. The results show that the product phases of the sintered alloys are AlFe, AlFe3, Al2O3, Al65Fe20W15, W and WO3. The sintered alloy exhibits batten organization, and with the increase of the laser sintering power, the battens get more homogeneous and even small. When the laser sintering power is up to 1 100 W, the sintered alloy achieves the maximum density of 4.47 g/cm3 and the minimum porosity of 4.43%; the highest hardness of the surface layer is 1 309.7HK, that of the middle layer is 1 003.1HK; the corrosion resistance is the best, the longest passivation area is 440 mV and the passivation current density is only 5.570 μA/mm2. When the laser sintering power gets to 1 000 W, the relative wear rate of the sintering alloy is the lowest, the abrasion rate of the surface layer is 0.06 mg/mm2 and that of the middle layer is 0.05 mg/mm2.

 

Key words: Fe-Al intermetallic compound; laser sintering; microstructure; property

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

主管:中國科學(xué)技術(shù)協(xié)會(huì) 主辦:中國有色金屬學(xué)會(huì) 承辦:中南大學(xué)
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