Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中國有色金屬學(xué)報(bào)

ZHONGGUO YOUSEJINSHU XUEBAO

第18卷    第7期    總第112期    2008年7月

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文章編號:1004-0609(2008)07-1261-07
MB8鎂合金陰極電沉積Ni-SiC納米復(fù)合鍍層微觀結(jié)構(gòu)及性能
李雪松1, 2,吳 化1,楊 友1,江中浩2

(1. 長春工業(yè)大學(xué) 材料科學(xué)與工程學(xué)院,長春 130012;
2. 吉林大學(xué) 汽車材料教育部重點(diǎn)實(shí)驗(yàn)室,長春 130025
)

摘 要:

采用以硫酸鎳為主鹽的電沉積技術(shù),在MB8形變鎂合金表面制備納米復(fù)合鍍層。利用掃描電鏡和透射電鏡觀察復(fù)合鍍層的顯微形貌和微觀結(jié)構(gòu),利用X射線衍射儀和能譜儀對復(fù)合鍍層進(jìn)行物相分析,利用顯微硬度計(jì)測定鍍層顯微硬度,利用快速磨損試驗(yàn)機(jī)測試復(fù)合鍍層的耐磨性能,利用電化學(xué)測試儀測定復(fù)合鍍層在3.5%NaCl(質(zhì)量分?jǐn)?shù))溶液中的極化曲線。結(jié)果表明:在MB8形變鎂合金表面可以獲得結(jié)晶均勻、結(jié)構(gòu)致密的納米復(fù)合鍍層,該復(fù)合鍍層的顯微硬度最高達(dá)HV 682,其耐磨性能超過硬鉻鍍層,且具有較好的耐蝕性能,自腐蝕電位較鎂合金基體提高677 mV。

 

關(guān)鍵字: MB8鎂合金;電沉積;納米復(fù)合鍍層;納米SiC

Microstructure and properties of cathode electrodeposited Ni-SiC nano composite coatings on MB8 magnesium alloy
LI Xue-song1, 2, WU Hua1, YANG You1, JIANG Zhong-hao2

1. College of Materials Science and Engineering, Changchun University of Technology, Changchun 130012, China;
2. Key Laboratory of Automobile Materials, Ministry of Education, Jilin University, Changchun 130025, China

Abstract:Nano composite coatings were prepared on MB8 wrought magnesium alloy by electrodeposition with sulfate nickel as main salt. The microstructure of the composite coatings were observed with scanning electron microscopy and transmission electron microscopy, its phase compositions were analyzed with X-ray diffractometry, its microhardness was determined with microhardness meter, its abrasive resistance was tested by rapid abrasive test, and its polarization curve in 3.5% (mass fraction) sodium chloride solution was determined by electrochemical tester. The results show that nano composite coatings with uniform crystalline, dense structure and better corrosion resistance can be obtained on MB8 wrought magnesium alloy and its maximum microhardness reaches HV 682. Moreover, the abrasive resistance of the composite coatings is superior to that of the hard chromium coating, the corrosion potential is increased by 677 mV compared with base Mg alloy.

 

Key words: MB8 magnesium alloy; electrodeposition; nano composite coating; nano-SiC

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

主管:中國科學(xué)技術(shù)協(xié)會(huì) 主辦:中國有色金屬學(xué)會(huì) 承辦:中南大學(xué)
湘ICP備09001153號 版權(quán)所有:《中國有色金屬學(xué)報(bào)》編輯部
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