中國(guó)有色金屬學(xué)報(bào)(英文版)
Transactions of Nonferrous Metals Society of China
| Vol. 21 No. 8 August 2011 |
combustion synthesis
（Key Laboratory for Ecological Utilization of Multimetallic Mineral of Ministry of Education,
Northeastern University, Shenyang 110004, China）
Abstract:High-purity, homogeneous and ultra fine LaB6 powders were prepared by combustion synthesis. The effects of reactant ratio and molding pressure on the phase and morphology of the combustion products were studied. The combustion products and leached products were analyzed by XRD, SEM and EDS. The results indicate that the combustion product consists of LaB6, MgO and a little Mg3B2O6. The combustion product becomes denser and harder when the molding pressure increases. The purity of LaB6 is higher than 99.0%. The LaB6 particle size is in range of 1.92–3.00 µm and the lattice constant of LaB6 is a=0.414 8 nm.
Key words: combustion synthesis; lanthanum hexaboride; Mg3B2O6
