Transactions of Nonferrous Metals Society of China The Chinese Journal of Nonferrous Metals

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中國(guó)有色金屬學(xué)報(bào)(英文版)

Transactions of Nonferrous Metals Society of China

Vol. 20    Special 1    May 2010

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Preparation and characterization of ultrafine zinc oxide powder by  hydrothermal method
SHEN Xiao-yi(申曉毅)1, ZHAI Yu-chun(翟玉春)1, ZHANG Yan-hui(張艷輝)2

1. School of Materials and Metallurgy, Northeastern University, Shenyang 110004, China;
2. Ningbo Institute of Technology, Zhejiang University, Ningbo 315100, China

Abstract:With Zinc acetate and sodium hydroxide as raw materials, while polyethylene glycol employed as dispersant agent, ultrafine zinc oxide powder was synthesized by hydrothermal method. Influence of NaOH concentration on morphology of ZnO powder was studied. The as-synthesized ZnO powder looked like flower cluster and consisted of microrods with hexagonal morphologies. The crystal structure and optical property of the as-prepared powder were also characterized using XRD, UV-visible absorption spectrum and photoluminescence spectrum. The results indicate that ZnO powder is of hexagonal wurtzite structure and well crystallized with high purity. There is a strong excitation absorption peak at 300 nm in UV-visible absorption spectrum and blue shift exists obviously. The optical property of ZnO powder is excellent.

 

Key words: zinc oxide; hexagonal wurtzite structure; photoluminescence spectrum; optical property

ISSN 1004-0609
CN 43-1238/TG
CODEN: ZYJXFK

ISSN 1003-6326
CN 43-1239/TG
CODEN: TNMCEW

主管:中國(guó)科學(xué)技術(shù)協(xié)會(huì) 主辦:中國(guó)有色金屬學(xué)會(huì) 承辦:中南大學(xué)
湘ICP備09001153號(hào) 版權(quán)所有:《中國(guó)有色金屬學(xué)報(bào)》編輯部
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